Synthesis of Polyamides by Direct Polycondensation with Diphenyl 2,3-Dihydro-2-oxo-3-benzothiazolyl Phosphate as a New Activating Agent

synthesis of new 2,3-diphenyl-3-oxo-propanamide derivatives as selective cox-2 inhibitors

Synthesis of new macrocyclic polyamides as antimicrobial agent candidates.

A series of macrocyclic imides and Schiff-bases have been prepared via the cyclocondensation of pyridine-2,6-dicarbonyl dichloride (1) with L-ornithine methyl ester to give the corresponding macrocyclic bisester 2. Treatment of 2 with hydrazine hydrate gave macrocyclic bisacid hydrazide 3, which was used as starting material. Condensation of bishydrazide 3 with diacid anhydrides or aromatic ald...

Synthesis of 5,6-Diphenyl-2,3-dihydro-1,2,4-triazine-3-thione as a New Reagent for Spectrophotometric Determination of Palladium

A new chromogenic reagent for the sensitive and selective determination of Pd ions in aqueous solution was synthesized. The reagent, 5,6-diphenyl-2,3-dihydro-1,2,4-triazine-3-thione, forms colored complexes with a few heavy metal ions. A 1:1 (M:L) yellowish orange colored complex of DPhDTT-Pd was formed in methanol. The molar absorptivity is 6.67×10 L mol cm. Bee’s law was obeyed in the concent...

Diethyl 2-oxo-3-(2-oxo-2,3-dihydro-1H-indol-3-yl­idene)butane­dioate

The title compound, C(16)H(15)NO(6), crystallizes with two symmetry-independent mol-ecules in the asymmetric unit. The crystal structure is stabilized by inter-molecular C-H⋯O and N-H⋯O hydrogen bonds, and intra-molecular C-H⋯O hydrogen bonds. In addition, the crystal structure exhibits two inter-molecular C-H⋯π inter-actions.

Facile Synthesis of Some 2-Alkyl-3-Aryl-5, 6-Diphenyl-2, 3-Dihydro-Pyrazines and their Biological Activity

The reaction of benzil, 1-alkyl-2-arylethanediamine dihydrochloride and sodium acetate trihydrate gave the target molecule dihydropyrazine derivatives 30-34. The compounds have been characterized on the basis of their FT-IR, 1H NMR and 13C NMR spectroscopies. All the compounds are screened for their antibacterial activity against Staphylococcus aureus, Klebsiella pneumoniae, Pseudomonas aerugin...